Identification
Name		9-Bromo-10-phenylanthracene
Synonyms		Anthracene,9-Bromo-10-phenyl 9-Bromo-10-phenylanthracene 10-phenyl-9-BroMoanthracene 9-Bromo-10-phenylant 10-broMo-9-phenylanthracene 9-bromo-10-phenylindole
Molecular Structure
Molecular Formula		C20H13Br
Molecular Weight		333.22
CAS Registry Number		23674-20-6
Properties
Density		1.393
Melting point		154-155 ºC
Boiling point		449.7±14.0 °C
Water Solubility		Insoluble in water. Soluble in hot toluene, dimethylformamide.
Appearence		light yellow powder
Purity		98%min
Safety Data
Safety Statements		24/25
HS Code		29039990

9-Bromo-10-phenylanthracene Preparation：

9-Phenylanthracene (2.5g, 9.83mmol) and NBS (2.1g, 11.8mmol) were dissolved in 80mL CHCl3. Then the mixture was heated to 60°C for 2h under N2. After cooled to room temperature, 20 mL water was added. And the mixture was extracted with CH2Cl2. The organic extracts were dried over anhydrous MgSO4 and concentrated by rotary evaporation.The crude product was recrystallized from methanol to get a green-yellow powder (2g, 61.2%). 1H NMR (500 MHz, CDCl3) δ 8.67 – 8.61 (m, 2H), 7.71 – 7.65 (m, 2H), 7.64 – 7.56 (m, 5H), 7.45 – 7.37 (m, 4H). EI-MS (m/z): Calculated for C20H13Br: 333.22. Found [M+]: 332.30.

Synthetic diagram of 9-bromo-10-phenylanthracene